dc.contributor.author |
Siqueira, Maria Carolina Bulhosa |
|
dc.contributor.author |
Gervini, Vanessa Carratu |
|
dc.contributor.author |
Oliveira, Leandro |
|
dc.contributor.author |
Locatelli, Aline |
|
dc.contributor.author |
Oliveira, Adriano Bof de |
|
dc.date.accessioned |
2014-09-24T03:24:43Z |
|
dc.date.available |
2014-09-24T03:24:43Z |
|
dc.date.issued |
2012 |
|
dc.identifier.citation |
SIQUEIRA, Maria Carolina Bulhosa et al. N' -[3-(Hydroxyimino)butan-2-ylidene]- 4-methylbenzene-1-sulfonohydrazide. Acta Crystallographica. Section E, v. 68, n. 3, p. 592, 2012. Disponível em:<http://scripts.iucr.org/cgi-bin/paper?S1600536812003339>. Acesso em: 23 set. 2014. |
pt_BR |
dc.identifier.issn |
1600-5368 |
|
dc.identifier.uri |
http://repositorio.furg.br/handle/1/4622 |
|
dc.description.abstract |
In the title compound, C11H15N3O3S, the C-S-N(H)-N linkage is nonplanar, the torsion angle being 75.70 (12)°. The compound has two almost planar fragments linked to the S atom: the hydrazone-derivative fragment [(HONC4H6)N-N(H)-] and the tolyl fragment (C7H7-) have maximum deviations from the mean plane through the non-H atoms of 0.0260 (10) and 0.0148 (14) Å, respectively. The two planar fragments make an interplanar angle of 79.47 (5)°. In the crystal, molecules are connected through inversion centers via pairs of N-H...O and O-H...N hydrogen bonds |
pt_BR |
dc.language.iso |
eng |
pt_BR |
dc.rights |
open access |
pt_BR |
dc.subject |
Single-crystal X-ray study |
pt_BR |
dc.subject |
T = 293 K |
pt_BR |
dc.subject |
Mean (C–C) = 0.002 A° |
pt_BR |
dc.subject |
R factor = 0.036 |
pt_BR |
dc.subject |
wR factor = 0.112 |
pt_BR |
dc.subject |
Data-to-parameter ratio = 18.5 |
pt_BR |
dc.title |
N' -[3-(Hydroxyimino)butan-2-ylidene]- 4-methylbenzene-1-sulfonohydrazide |
pt_BR |
dc.type |
article |
pt_BR |
dc.identifier.doi |
10.1107/S1600536812003339 |
pt_BR |